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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 5 of 24  Not logged in ELOG logo
ID Date Authordown Group Subject
  308   17 Aug 2023, 11:07 Teguh Citra Asmara, Eugenio ParisSCSMorning Shift Summary on 16.08.2023

Achievements:

  1. Performed tr-RIXS on peak A, B, and C at 2.4 mJ/cm^2
  2. Performed tr-XAS on peak A at 3 fluences
  3. Performed tr-RIXS on peak A at 4 mJ/cm^2

Problems:

  1. BAM delay line compensator was not working due to incorrect macro. DOC and LM fixed the issue.
  2. Delay line scan of hRIXS camera was not working as it was still configured for Viking. MT fixed the issue.
  3. The new centroiding algorithm (provided natively by the 4137 kernel) is not consistent with integration mode. For the time being, we use an older, manually configured centroiding algorithm developed for a previous user beamtime.
  4. tR-XAS results show large changes, but these large changes were not reflected in tr-RIXS.
  309   17 Aug 2023, 11:08 Teguh Citra AsmaraSCSAfternoon shift summary on 16.08.2023

Achievements:

  1. tr-RIXS at 4 mJ/cm2 for energies A, B, C, and D (pre-edge)
  2. Checked and optimized FEL alignment, t0 and overlap with PP laser after reset of machine synchronization
  3. Long delay scans for Peak A and C, up to 100 ps
    Problems:

  4. Need to reset machine synchronization by BKR

  5. Camera scene got stuck, was resolved by DOC

  138   16 Apr 2023, 15:35 Silja SchmidtchenXROShift summary

shift summary from Saturday 15.04.2023:

Tasks:

- Calibration of Euler MDL

- Vibrometer measurements at M3 using the RY piezo

Beam was aligned to MID popin

we used values stored in MID setpoints 'B' but went there manually, using the EulerMDL

M1 - X value was corrected, as we found the center of the beam/mirror to be at 6.4mm - calculated beam angle after M1 is 2.14mrad

M2 - values slightly differ from saved setpoints but were quite well met using EulerMDL to reach the same beam position

M3 - we had to remove it a bit further from the beam, as it seemed to intercept it, when we first tried to get the beam through. This might in the end not have been necessary

End of shift:

beam aligned to MID

preabsorber in

SRA fully open

  272   21 Jul 2023, 20:31 Silja SchmidtchenXROShift Summary SA2

Alignment to HED: https://in.xfel.eu/elog/XRO+Beam+Commissioning/205

SA2 - divergence with various M2 bender positions  HED - https://in.xfel.eu/elog/XRO+Beam+Commissioning/200

SA2 - divergence with various M2 bender positions MID - https://in.xfel.eu/elog/XRO+Beam+Commissioning/196

Issues with HED PBLM blade in SA2: https://in.xfel.eu/elog/XRO+Beam+Commissioning/195

Vobration measurements could not be done https://in.xfel.eu/elog/XRO+Beam+Commissioning/207

End of shift:

SA2 left with preAbs in

machine wanted to increase intensity

  414   25 Oct 2023, 15:10 Sergii, TeguhSCSMorning Shift Summary, 24.10.2023

Morning Shift Summary, 24.10.2023

Achievements:

  1. Re-aligned the beamline after maintenance
  2. Found time zero using SiN at 300 K
  3. Change the He dewar and cooled down back to 20 K
  4. Adjusted the AFS laser parameters to recover the proper experiment settings
  5. Started taking tr-RIXS with several time delay points

Problems:

  1. The AFS laser power is smaller than last week

Next shift plan:

  1. Continue taking tr-RIXS data
  415   25 Oct 2023, 15:18 Sergii, TeguhSCSMorning Shift Summary, 25.10.2023

Morning Shift Summary, 25.10.2023

Achievements:

  1. Re-aligned FEL beam pointing and beamline mirrors after XGM intensity drop due to slow beam pointing drift over night.
  2. Continued taking momentum-dependent tr-REXS data.

Problems:

  1. There was slow drift of FEL beam pointing over night, causing XGM intensity to slowly drop over time.
  2. The slow drop of XGM intensity continues even after beamline alignment. Compared to morning, the XGM intensity has dropped by ~10%.
  3. It is advisable to re-check the beam pointing again some time before the night shift due to correct for this beam drift problem.
  418   26 Oct 2023, 15:03 Sergii, TeguhSCSMorning shift summary, 26.10.2023

Morning shift summary, 26.10.2023

Achievements:

  1. Continued measuring tr-RIXS at different laser fluences

Problems:

  1. The max-jhub notebook server was very slow this morning around 9-10 h. DOC was informed, but the slowness has improved without any action from either them or our side. The reason for this slowness is still unknown, but the max-jhub server has come back to normal for now.
  175   04 May 2023, 22:58 Sergii, PhuongSCSLate shift summary 04.05.2023

Achivements:

-Cooling down the sample. Sample is at 14K

-Taking time resolved data at 70%  800 nm, -5 ps  - 65 ps

Problems

-Freezing of the transfer line while cooling. It seems the scroll pump was brocken. When we replace the pump cooling was OK.

  183   05 May 2023, 23:00 Sergii, PhuongSCSLate shift summary 05.05.2023

Achivments:

-Measure time scans with magnetic field in opposite directions

Problems

-At some point data analysis was imposible. No reseurses could be dedicated for the analysis. We switch both AMORE and offline analysis to nodes, dedicated for the proposal.

-We found very slow drift of xray intensity at XGM. It was becasue x-ray pointing was slightly changed. We restore the pointing with M2 pitch motor

  189   06 May 2023, 23:15 Sergii, PhuongSCSLate shift summary 06.05.2023

Achivments:

-Measure delay scans at two PPL fluencies on smaller grain size.

-Moved DSSC back to 1.45 m sample - detector distance

Problems

-No major problems

  193   07 May 2023, 23:11 Sergii, PhuongSCSLate shift summary 07.05.2023

Achivments:

-Move DSSC closer to the sample.

-Measure delay scans for opposite magnetic field.

Problems:

-No major problems

  62   01 Mar 2023, 23:31 Sergii, MartinSCSLate shift summary 01.03.2023

Achievments:

- Align DPS to remove clipping of X-rays

- Get better focusing of PPL in the chamber

-Coarse timing with SIGNAl of OPA

-Switch back to 3 um PPL settings

Problems

-It was hard to work with DPS without motorized stages

 

  284   31 Jul 2023, 01:42 Sergii, MartinSCSNight shift summary 30.07.2023

Achivements:

-We measured vertical spot size for several VFM settings

Problems:

-We cannot focus the x-ray beam with KB. The best value what we can get is ~300 um. We checked the slits of KB. The ALAS is slightly clipped on parabolic mirror of tim ing chamber. TI is not clear if this is the reason. We cannot proceed with the program for hRIXS.

-Still no signal on APD.

  275   28 Jul 2023, 06:38 Sergii, ManuelSCSShift Summary 27_07_23 night

Achievements:

1. Beam in sample chamber, almost overlapping with ALAS

2. We saw signal on MCP and diode2

3. Sample Motors aligned close to the desired height in chamber

 

Problems:

1. Slow response of Screens and mirror motors, solved by restarting the Beckhoff of the mirror motors

2. Could not find signal of unfocused beam on SCS Pop-In

3. Acquiring data with the spectrometer for energy calibration does not work

4, Motor STZ of XRD does not allow halfclip of the beam.

5. No Fluorescence signal on the APD

6. In the DAQ we can not execute "assign" or "cofigure" action

  313   19 Aug 2023, 07:16 Sergii, ManuelSCSNoght shift sammary 18.08.2023

Night shift summary on 18.03.2023

  1. Finished XAS series at 1.5 mJ/mm² for different delays
  2. Performed XAS at 6 mJ/mm²
  3. Tested tr-RIXS signal at 1mj/mm² with 29 different delays, signal too weak to continue
  4. Took 5 hours of tr-RIXS signal at 1.2 mj/mm² with 29 different delays

Problems:

  1. Something in the cryo line froze, cleaned the line by going into the hutch and moving the needle valve a bit. This only helped short-term, as it kept freezing after short time.
  2. Temperature sensor at the sample stopped working, started to work again during the heating
  398   20 Oct 2023, 23:22 Sergii, GiacomoSCSLate Shift Summary on 20.10.2023

Late shift summary 20.10.2023

Achievements
-Switched AFS to burst mode
-Characterized PPL beam size
-Found coarse timing
-Working on fine timing with TR_XAS
Problems
-SCS_XGM data recorded with some mismatch that the run could not be loaded for an offline analysis with XGM. Other channels are fine.

  401   21 Oct 2023, 23:34 Sergii, GiacomoSCSLate shift summary 21.10.2023

Achievements:
-Collecting TR-RIXS data for different fluencies and delay range
Problems
-No major problems

  72   04 Mar 2023, 23:04 Sergii, AndreasSCSlate shift summary

Achievements:

- we replaced broken SMA cable, and added an angle-connector at sample holder to aid the sample rotation when moving diagnostics to the flat jet

- we double-checked coarse timing and x-ray beam size

- we found t0 on SiN

- setting up RIXS with time delay steps for the night shift program

 

 

 

 

  73   05 Mar 2023, 23:04 Sergii, AndreasSCSLate shift summary 05.03.2023

Achievments

-RIXS scans at different delay times and x-ray energies

-Cross check fine timing

Problems

-Nozzle was frozen. Pump was in error state.

  290   05 Aug 2023, 23:06 Sergii, AndreasSCSLate shift summary 05.08.2023

Achievements:

- Find course timing with antenna

-Find find timing signla with TR_XAS on the sample

-Measure XAS with laser ON and OFF to find optimal conditions for TR study

-Measure TR_XAS at low T

Problems:

-temperature went up and the cooling was not responing to the change of needle valve. When we tweak a bit transfer line needle valve cooling starts again.

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