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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 21 of 24  Not logged in ELOG logo
Entry   Shift summary, posted by Chan Kim on 26 Oct 2023, 07:10 
X-ray delivery


7.8keV, 2.4mj, stable delivery, homogeneos intra train energy most of the time.


Optical laser delivery


ns laser for particle imaging


Achievements/Observations
Entry   Issue, posted by Chan Kim on 27 Oct 2023, 03:19 Screenshot_from_2023-10-27_03-09-25.png
We observed auto changes of the number of X-ray pulses last night and tonight.

It is related to 500 um thick Si attenuator in XTD2_ATT.

Even with 2.4 mm thick CVD (XTD2_ATT) IN, the number of pulses @SA1 changes to 28 whenever we insert 500 um thick Si attenuator.
Entry   Shift summary, posted by Chan Kim on 27 Oct 2023, 06:35 
X-ray delivery


7.8keV, 2.5mj, stable delivery, homogeneos intra train energy most of the time.


Optical laser delivery


ns laser for particle imaging


Achievements/Observations
Entry   Shift summary, posted by Chan Kim on 31 Oct 2023, 23:08 
X-ray delivery


19keV, 700-800uj


Optical laser delivery


 ns laser


Achievements/Observations
Entry   Shift summary, posted by Chan Kim on 01 Nov 2023, 22:57 
X-ray delivery


19 keV, ~0.9 mJ/pulse, stable delivery


Optical laser delivery


 no


Achievements/Observations
Entry   Shift summary, posted by Chan Kim on 02 Nov 2023, 23:25 
X-ray delivery


19 keV, ~0.9 mJ/pulse, stable delivery


Optical laser delivery


 no


Achievements/Observations
Entry   other, posted by Chan Kim on 24 Nov 2023, 20:48 Screenshot_from_2023-11-24_20-42-17.pngScreenshot_from_2023-11-24_20-42-08.png
Beam drift in the horizontal direction (XTD9_XGM x position) started at around 10am and continuously drifted until 16:00.

After then, beam has been drifted back to original position within 4 hours.
Entry   Shift summary, posted by Chan Kim on 24 Nov 2023, 23:11 
X-ray delivery


16.9 keV, up to 30 pulses and 1.1 MHz for alignment, 1 pulse for data collection
900 uJ
Beam pointing and stability
issues towards end of shift


Optical laser delivery
Entry   other, posted by Chan Kim on 25 Nov 2023, 19:56 Screenshot_from_2023-11-25_19-54-18.png
Beam drift in the horizontal direction (XTD9_XGM).

From ~16:00, X-ray beam started to drift in the horizontal direction. In total, ~0.3 mm drift observed within 2-3 hours.

 
Entry   Shift summary, posted by Chan Kim on 25 Nov 2023, 23:45 
X-ray delivery


16.9 keV, up to 30 pulses and 1.1 MHz for alignment, 1 pulse for data collection
800 uJ
Beam pointing and stability
issues towards end of shift (again)


Optical laser delivery
Entry   Sample Camera got stuck (likely at 11pm) and was only noticed at 5am, posted by Bjoern Senfftleben on 24 Nov 2023, 05:07 Screenshot_from_2023-11-24_05-01-47.pngScreenshot_from_2023-11-24_05-09-07.pngScreenshot_from_2023-11-24_05-18-07.png
After going in and reconnecting the camera, we observe att. 1.

 

According to logs the camera device server was restarted around 11pm, however the camera instance was never reinstantiated after the restart.
Entry   Late Shift Summary, posted by Benjamin, Yi-Ping, Ru-Pan, Andreas on 31 Mar 2023, 05:10 
Achievements


Optimized BOZ for Co and Fe
Estabilished Stable liquid jet flow with 30 mM Fe(bpy)3


Problems


Jet froze several times
Chamber warmed up earlier in the day. This led to a "dusting" of CNCbl on many surfaces
Entry   Shift Summary, posted by Benjamin, Robert, Yi-Ping, Ru-Pan on 30 Mar 2023, 04:16 
Achievements


Found coarse timing between XFEL and optical laser


Problems


Did not see a observe fine timing signal from silicon nitride measurement


Plan for night shift
Entry   morning shift summary, posted by Benjamin, Nahid, Raphael, Philippe, Victoria, Timo on 15 Mar 2023, 17:01 
Achievements


Found RIXS signal from liquid jet
Measured static RIXS and PFY-XAS spectrum of Co(cp)(CO)2


Problems


hRIXS detector has a data latency issue and images were not being recorded in the DAQ. This required ~2-3 hours to solve plus time lost
Entry   Night Shift summary, posted by Benjamin, Manuel, Ricardo on 18 Feb 2023, 07:06 
Achievements


Used scanning of liquid jet to improve S/N
Measured x-ray PP XAS as a function of the delay between the two X-ray colors
Scan
energy of probe pulse with fixed pump energy


Problems
Entry   Night Shift Summary, posted by Benjamin van Kuiken on 15 Feb 2023, 06:54 
Achievements


Located flat jet and attempted measurement of XAS at several incident energies 1300, 1305, 1315 eV


Problems


 We have difficulty locating the beam on the sample

We have not found a signal on eith of the diodes in the Chem chamber.
Knife
Entry   Late Shift Summary, posted by Benjamin van Kuiken on 02 Apr 2023, 04:46 
Achievement


Measured tXAS at the Fe L-edge of Fe(bpy)3 using both delay and energy scans. 


Issues


The cold traps ran empty on the chamber resulting in a pressure spike that interlocked the DSSC
The rough vacuum of the chem
Entry   Shift summary, posted by Benjamin van Kuiken on 22 Sep 2023, 06:51 
Achievemnets


Characterized the X-ray and laser danage on the STO2LNO2


Problems


Cound not find fine timeing from XAS measurements performed on the sample

MCP sees 266 nm PP laser
SiN mesaurement
Entry   SCS Night Shift Summary, posted by Benjamin van Kuiken on 27 Sep 2023, 07:51 SCSPopinOthOrder_270923.png
Achievements


Characterized optical laser spot at sample


Problems


FEL beam had very unstable intensity and spectrum. As a result no useful data could be collected during the night

FEL pointing
Entry   Morning Shift Summary, posted by Benjamin van Kuiken on 20 Oct 2023, 15:22 
Achievements


Tested MCPs and APD for XAS

Both MCPs give a good XAS spectrum with no amplification, but small MCP requires higher bias
voltage
No fluorescence signal observed on the APD


Measured XAS of both samples
Measured static RIXS
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