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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 5 of 24  Not logged in ELOG logo
Entry   Morning Shift Summary on 16.08.2023, posted by Teguh Citra Asmara, Eugenio Paris on 17 Aug 2023, 11:07 

Achievements:

  1. Performed tr-RIXS on peak A, B, and C at 2.4 mJ/cm^2
  2. Performed tr-XAS on peak A at 3 fluences
  3. Performed tr-RIXS on peak A at 4 mJ/cm^2

Problems:

  1. BAM delay line compensator was not working due to incorrect macro. DOC and LM fixed the issue.
  2. Delay line scan of hRIXS camera was not working as it was still configured for Viking. MT fixed the issue.
  3. The new centroiding algorithm (provided natively by the 4137 kernel) is not consistent with integration mode. For the time being, we use an older, manually configured centroiding algorithm developed for a previous user beamtime.
  4. tR-XAS results show large changes, but these large changes were not reflected in tr-RIXS.
Entry   Afternoon shift summary on 16.08.2023, posted by Teguh Citra Asmara on 17 Aug 2023, 11:08 

Achievements:

  1. tr-RIXS at 4 mJ/cm2 for energies A, B, C, and D (pre-edge)
  2. Checked and optimized FEL alignment, t0 and overlap with PP laser after reset of machine synchronization
  3. Long delay scans for Peak A and C, up to 100 ps
    Problems:

  4. Need to reset machine synchronization by BKR

  5. Camera scene got stuck, was resolved by DOC

Entry   Shift summary, posted by Silja Schmidtchen on 16 Apr 2023, 15:35 

shift summary from Saturday 15.04.2023:

Tasks:

- Calibration of Euler MDL

- Vibrometer measurements at M3 using the RY piezo

Beam was aligned to MID popin

we used values stored in MID setpoints 'B' but went there manually, using the EulerMDL

M1 - X value was corrected, as we found the center of the beam/mirror to be at 6.4mm - calculated beam angle after M1 is 2.14mrad

M2 - values slightly differ from saved setpoints but were quite well met using EulerMDL to reach the same beam position

M3 - we had to remove it a bit further from the beam, as it seemed to intercept it, when we first tried to get the beam through. This might in the end not have been necessary

End of shift:

beam aligned to MID

preabsorber in

SRA fully open

Entry   Shift Summary SA2, posted by Silja Schmidtchen on 21 Jul 2023, 20:31 

Alignment to HED: https://in.xfel.eu/elog/XRO+Beam+Commissioning/205

SA2 - divergence with various M2 bender positions  HED - https://in.xfel.eu/elog/XRO+Beam+Commissioning/200

SA2 - divergence with various M2 bender positions MID - https://in.xfel.eu/elog/XRO+Beam+Commissioning/196

Issues with HED PBLM blade in SA2: https://in.xfel.eu/elog/XRO+Beam+Commissioning/195

Vobration measurements could not be done https://in.xfel.eu/elog/XRO+Beam+Commissioning/207

End of shift:

SA2 left with preAbs in

machine wanted to increase intensity

Entry   Morning Shift Summary, 24.10.2023, posted by Sergii, Teguh on 25 Oct 2023, 15:10 

Morning Shift Summary, 24.10.2023

Achievements:

  1. Re-aligned the beamline after maintenance
  2. Found time zero using SiN at 300 K
  3. Change the He dewar and cooled down back to 20 K
  4. Adjusted the AFS laser parameters to recover the proper experiment settings
  5. Started taking tr-RIXS with several time delay points

Problems:

  1. The AFS laser power is smaller than last week

Next shift plan:

  1. Continue taking tr-RIXS data
Entry   Morning Shift Summary, 25.10.2023, posted by Sergii, Teguh on 25 Oct 2023, 15:18 

Morning Shift Summary, 25.10.2023

Achievements:

  1. Re-aligned FEL beam pointing and beamline mirrors after XGM intensity drop due to slow beam pointing drift over night.
  2. Continued taking momentum-dependent tr-REXS data.

Problems:

  1. There was slow drift of FEL beam pointing over night, causing XGM intensity to slowly drop over time.
  2. The slow drop of XGM intensity continues even after beamline alignment. Compared to morning, the XGM intensity has dropped by ~10%.
  3. It is advisable to re-check the beam pointing again some time before the night shift due to correct for this beam drift problem.
Entry   Morning shift summary, 26.10.2023, posted by Sergii, Teguh on 26 Oct 2023, 15:03 

Morning shift summary, 26.10.2023

Achievements:

  1. Continued measuring tr-RIXS at different laser fluences

Problems:

  1. The max-jhub notebook server was very slow this morning around 9-10 h. DOC was informed, but the slowness has improved without any action from either them or our side. The reason for this slowness is still unknown, but the max-jhub server has come back to normal for now.
Entry   Late shift summary 04.05.2023, posted by Sergii, Phuong on 04 May 2023, 22:58 

Achivements:

-Cooling down the sample. Sample is at 14K

-Taking time resolved data at 70%  800 nm, -5 ps  - 65 ps

Problems

-Freezing of the transfer line while cooling. It seems the scroll pump was brocken. When we replace the pump cooling was OK.

Entry   Late shift summary 05.05.2023, posted by Sergii, Phuong on 05 May 2023, 23:00 

Achivments:

-Measure time scans with magnetic field in opposite directions

Problems

-At some point data analysis was imposible. No reseurses could be dedicated for the analysis. We switch both AMORE and offline analysis to nodes, dedicated for the proposal.

-We found very slow drift of xray intensity at XGM. It was becasue x-ray pointing was slightly changed. We restore the pointing with M2 pitch motor

Entry   Late shift summary 06.05.2023, posted by Sergii, Phuong on 06 May 2023, 23:15 

Achivments:

-Measure delay scans at two PPL fluencies on smaller grain size.

-Moved DSSC back to 1.45 m sample - detector distance

Problems

-No major problems

Entry   Late shift summary 07.05.2023, posted by Sergii, Phuong on 07 May 2023, 23:11 

Achivments:

-Move DSSC closer to the sample.

-Measure delay scans for opposite magnetic field.

Problems:

-No major problems

Entry   Late shift summary 01.03.2023, posted by Sergii, Martin on 01 Mar 2023, 23:31 

Achievments:

- Align DPS to remove clipping of X-rays

- Get better focusing of PPL in the chamber

-Coarse timing with SIGNAl of OPA

-Switch back to 3 um PPL settings

Problems

-It was hard to work with DPS without motorized stages

 

Entry   Night shift summary 30.07.2023, posted by Sergii, Martin on 31 Jul 2023, 01:42 

Achivements:

-We measured vertical spot size for several VFM settings

Problems:

-We cannot focus the x-ray beam with KB. The best value what we can get is ~300 um. We checked the slits of KB. The ALAS is slightly clipped on parabolic mirror of tim ing chamber. TI is not clear if this is the reason. We cannot proceed with the program for hRIXS.

-Still no signal on APD.

Entry   Shift Summary 27_07_23 night, posted by Sergii, Manuel on 28 Jul 2023, 06:38 

Achievements:

1. Beam in sample chamber, almost overlapping with ALAS

2. We saw signal on MCP and diode2

3. Sample Motors aligned close to the desired height in chamber

 

Problems:

1. Slow response of Screens and mirror motors, solved by restarting the Beckhoff of the mirror motors

2. Could not find signal of unfocused beam on SCS Pop-In

3. Acquiring data with the spectrometer for energy calibration does not work

4, Motor STZ of XRD does not allow halfclip of the beam.

5. No Fluorescence signal on the APD

6. In the DAQ we can not execute "assign" or "cofigure" action

Entry   Noght shift sammary 18.08.2023, posted by Sergii, Manuel on 19 Aug 2023, 07:16 

Night shift summary on 18.03.2023

  1. Finished XAS series at 1.5 mJ/mm² for different delays
  2. Performed XAS at 6 mJ/mm²
  3. Tested tr-RIXS signal at 1mj/mm² with 29 different delays, signal too weak to continue
  4. Took 5 hours of tr-RIXS signal at 1.2 mj/mm² with 29 different delays

Problems:

  1. Something in the cryo line froze, cleaned the line by going into the hutch and moving the needle valve a bit. This only helped short-term, as it kept freezing after short time.
  2. Temperature sensor at the sample stopped working, started to work again during the heating
Entry   Late Shift Summary on 20.10.2023, posted by Sergii, Giacomo on 20 Oct 2023, 23:22 

Late shift summary 20.10.2023

Achievements
-Switched AFS to burst mode
-Characterized PPL beam size
-Found coarse timing
-Working on fine timing with TR_XAS
Problems
-SCS_XGM data recorded with some mismatch that the run could not be loaded for an offline analysis with XGM. Other channels are fine.

Entry   Late shift summary 21.10.2023, posted by Sergii, Giacomo on 21 Oct 2023, 23:34 

Achievements:
-Collecting TR-RIXS data for different fluencies and delay range
Problems
-No major problems

Entry   late shift summary, posted by Sergii, Andreas on 04 Mar 2023, 23:04 

Achievements:

- we replaced broken SMA cable, and added an angle-connector at sample holder to aid the sample rotation when moving diagnostics to the flat jet

- we double-checked coarse timing and x-ray beam size

- we found t0 on SiN

- setting up RIXS with time delay steps for the night shift program

 

 

 

 

Entry   Late shift summary 05.03.2023, posted by Sergii, Andreas on 05 Mar 2023, 23:04 

Achievments

-RIXS scans at different delay times and x-ray energies

-Cross check fine timing

Problems

-Nozzle was frozen. Pump was in error state.

Entry   Late shift summary 05.08.2023, posted by Sergii, Andreas on 05 Aug 2023, 23:06 

Achievements:

- Find course timing with antenna

-Find find timing signla with TR_XAS on the sample

-Measure XAS with laser ON and OFF to find optimal conditions for TR study

-Measure TR_XAS at low T

Problems:

-temperature went up and the cooling was not responing to the change of needle valve. When we tweak a bit transfer line needle valve cooling starts again.

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