Like after the previous winter maintenance period, the shutter of FXE appears as opened in DOOCS panels even though it is closed (https://in.xfel.eu/elog/OPERATION-2023/58).

shift summary
Andreas, Giuseppe

• continued pumpprobe measurements
• around 5:30 we could not see any image at the MTE3 camera (after sample transfer), we tried to fix it but did not work
• we tried to remove the samples from the LLC, the LLC is vented but the lift cannot be moved, needs to be repaired during the day.

X-ray delivery

• 1-350 at 12.45 keV, 1600 uJ. Stable delivery

Optical laser delivery

• None

Achievements/Observations

• collected data at different delay times 20s and 40s
• we installed new mixing injector to allow for longer delay times; and collected complete dataset with it
• completed four different delay times for the users 14s, 18s, 20s and 40s

Issues

• spent longer times to make stable jet which cause many interruptions and hutch searches almost every 5 mins for several hours.
• it was extremely difficult to mix with delay at 20s with original setup.
• nozzles broken during the day, costing several hours to prepare new ones

X-ray delivery
1-350 at 12.45 keV, 1700 uJ. Stable delivery

Optical laser delivery

None

Achievements/Observations

- collected data at different delay times 14s and 18s with over 7 hours of data collection
- the jet was stabilized again by removing the catcher and decreasing transmission to ~30%
- removing the catcher is critical to get stable jet, that allowed us to run for over 20 runs without stop.

Issues

- The jet was extremely unstable for 1.5 shifts; we needed to stop the runs intermittently with intervals less than 10 mins. 
- It seems difficult in principle to go for longer delay times with the current setting; may be elongating the distance in Y-axis with 400 pixel if the jet stable may help to reach 20s.

Night shift summary
Andreas, Giuseppe

• we finished to measure sample 17 and 41 in CARD 06_Y2018F04
• we transferred sample Card_07_Y2018F19
• we started measuring sample 500 nm Ti #26

Problems:

• the frame could not be grabbed properly from the transfer arm, so we decide to vent and transfer manually
• we realized that FEL beam drifted horizontally, we corrected by moving M2 pitch. (The beam did not move at XGM in XTD10, so it must have been some mirror movement)

X-ray delivery

• 1-350 at 12.45 keV, 1750 uJ. Stable delivery

Optical laser delivery

Achievements/Observations

• completed Uwe and Petra data.
• the jet is almost established for <mixing experiments

Issues

X-ray delivery

• 1-350 at 12.45 keV, 1700 uJ. Stable delivery

Optical laser delivery

• None

Achievements/Observations

• collected about over 15 hours of quality data from different samples (thanks to FXE) with extremely stable jet.

Issues

• Issue with data processing in the morning and from the day before due to DAQ; only half of the detector data were calibrated; this was solved by switching to the old DAQ

X-ray delivery

• 1-350 at 12.45 keV, 1700 uJ. Stable delivery

Optical laser delivery

• None

Achievements/Observations

• fixing many issues with the cube and helium leaks
• collected many quality diffraction data for both jet with and without samples
• data on Nendu mutant (~2.5 hours of data collection) with two different conditions

Issues

• AGIPD data aggregator stopped responding and it took about 1 h to be fixed by DOC, which interrupted the data collection

• some strange streak diffraction appears on JF4M and this has to be removed by scanning X- and Y- nozzle motors carefully

Late shift 07.02.24
Laurent, Martin

Continued with laser preparation

• optimized SHG
• changed lens to f = 600 mm
• knife edge scans
• found optimum lens position (95 mm) for w0 = 70 um
• fluence characterization --> up to more than 2 J /cm^2
• Coarse timing
• Fine timing

night shift summary 07.02.24

Andreas, Giuseppe

program was to determine horizontal an vertical beam size and then create some single laser shot patterns to determine fluence settings for LIPSS.

PROBLEMS:

• knife edge insensitive to beam sizes smaller than 20um due the large beam jitter of the FEL.
• moved to the camera and curved gratings but then encountered vacuum issue with scroll pump down since noon 07.02. fixed by replacing scroll pump.
• useful camera data could not extracted as we cannot control the TPI shutter and have multiple exposures of the camera. STPulser Macro need to be fixed.
• SCS_XTD10_TPI/DCTRL/SHUTTER in the SCS topic is not found after shutting device down when tracking down device issues.

check of the optimized focussing options at 10 keV using only one arm in CRL2 - results still to be evaluated
successful check of the mirror chamber in the experiment hutch of MID - it was possible to reflect the direct beam down and use it under a shallow angle on the sample position

Goal Achieved.
- Finished flat field measurement for AGIPD at different scenarios for upcoming user experiments. 
- Aligned the spectrometer at DES and obtained the energy spectrum of 9 keV SASE.
- In order to investigate the sample to detector distance of AGIPD, we collected SAXS patterns from three different type of SiO2 NPs at different sample positions.
- Finished preparations for tomorrow.
 

goals achieved:
alignment of the beam in tunnel and hutches including refinement of the beam in the center of rotation 
check of cameras and optical components
initial check of the mirror chamber (successfully)

issues:
smarACT motors in the DES tricky - some are in error state and the filter wheel is moving and does not stop - positioned it and removed afterwards the cable - EEE intervention next week necessary
camera of Pop-in imager II45-2 in XTD6 went into error - DOC solved the issue

X-ray delivery

• 1-64 pulses at 10 keV, ~1.1 mJ.
• Overall stable delivery.

Optical laser delivery

• NA

Achievements/Observations

• Measured flat fields for JUNGFRAU for all configurations. Detector program completed.

Issues

• Mishap of lit frame finder with custom bunch patter.
• Apparent issue to process JUNGFRAU darks caused by lack of disk space. Solved by DOC/CAL.
• Ghost run in myMdC upsetting the run controller. Solved by DOC and cause under further investigation.

beam parametes: 8.5-9 kev, 1.2 mJ, 1-2 pulses

• HED trajectory established from XRO setpoint, shape and transmission optimized
• monochromator aligned
• 5 sets of CRLs including nano-focus aligned
• ZZ yesterday morning to fix cameras, connect motors..
• DAQ rolled back to legacy version, works fine
• instrument spectrometers aligned and calibrated
• We perform some longer scans with monochromated beam imaging on wires / Siemens star
• Work on shimadzu timing
• Debugging new JNGFR_DARK_CHAR middle layer with controls - done

X-ray delivery

• 1-352 pulses at 10 keV, 1200 - 400 uJ.
• Significant pulse energy slope within the train. Action on the kickers was eventually performed leading to some reduction of the slope, though remaining still far from ideal. Decision to take the action took a very long time (2.5 hours).
• Several beam delivery interruptions through the afternoon due to trips of A16 before is was taken off beam.
• At 21:29:20, the number of bunches in SASE1 was changed from 1 to 352 without intervention of the SPB/SFX shift crew resulting in the destruction of a sample (see elog:7).

Optical laser delivery

• 800 nm, 50 fs, 1-113 pulses at 564 kHz.
• Brief intensity and spectral fluctuations as already observed in the past with non-optimal AMPHOS regulation. Detail will be communicated to LAS.

Achievements/Observations

• Measured flat fields for AGIPD for all remaining configurations.
• Confirmed timing of JUNGFRAU.
• Established pump-probe timing at IRDa.

Issues

• Several issues with AGIPD controls: timeout when trying to stop sending data, two hemispheres in different states, etc. Experts informed.
• Destruction of the sample following number of pulses incident in the evening caused a considerable loss of time to replace the sample and resume operation.
• XTD2 500 um Si is damaged (leftover from last run).

At 21:29:20 today, the number of bunches in SASE1 was increased from 1 to 352 without intervention of the SPB/SFX shift crew. 30 seconds later, the number of bunches was reduced to 1, again without intervention from the SPB/SFX shift crew (see attachments 1 and 2).

We were in the middle of a measurement at that time and the sudden increase from 10 mW to 3.5 W average power resulted in the destruction of the sample we were using.

AGIPD and JUNGFRAU are safe and were not at risk at the time of the incident, but this is merely by luck.

The origin of the change in number of bunches is unclear to us and needs to be investigated. It goes without saying that this is extremely dangerous for equipment and the damages could have been even worse.

Moning shift summary (31.01 and 01.02)

Acievements:
- SRA recalibrated, cross position on FEL imager found
- VSLIT in SA3 check calibration
- LEPM angle changed for LRGR. Calibration of photon energy server done with help of Ne in GATT.
- Several configurations for SCS have been adjusted/established
 

31.01.2024 (Day shift)

X-ray delivery

• 10 keV
• 1200 - 400 uJ (significant pulse energy slope within train)

Optical laser delivery

• None

Achievements/Observations

• Flat fields and timing scans were measured for AGIPD (1.1MHz, normal CDS mode)

Issues

• Interlocks issue causing beam to be interrupted when the beamline shutter was open https://mylog.connect.xfel.eu/#narrow/stream/111-SPB_900429_RichardBean/topic/Issues/near/32289
• Opening EXP hutch gate valves resulted in vacuum issue https://mylog.connect.xfel.eu/#narrow/stream/111-SPB_900429_RichardBean/topic/Alignment/near/32195
• Pulse pattern decoder recorded empty arrays, even though data were visible in Karaboo https://mylog.connect.xfel.eu/#narrow/stream/111-SPB_900429_RichardBean/topic/Issues/near/32299
• AGIPD timing issue caused by the wrong Trigger Source https://mylog.connect.xfel.eu/#narrow/stream/111-SPB_900429_RichardBean/topic/Detector.20Status/near/32408

To do for next shift

• Continue with the detector program