X-ray delivery

• 7.0 keV, up to 202 pulses at 564 kHz, ~1.7 mJ.
• Number of pulses initially limited to 178. Promptly addressed by BKR.

Optical laser delivery

• 800 nm, up to 202 pulses at 564 kHz.
• Oscillating wavelength due to known faulty DMBCC stage, but otherwise stable delivery.

Achievements/Observations

• Aligned instrument and collected data with test samples as well as various background signals in preparation for next suer experiment.

Issues

• Changing the ROI of a Zyla appears to affect its timing.

X-ray delivery

• 7.0 keV, up to 202 pulses at 564 kHz, 1.6-1.9 mJ.
• Average pulse energy tuned up to 1.9 mJ at 14:45, but slow continuous decay after that down to 1.7 mJ at the end of the shift.
• 45 minutes downtime in the morning and another 15 minutes to reset the IBFB later on, as coordinated by the PRC.

Optical laser delivery

• 800 nm, up to 202 pulses at 564 kHz.
• Large intensirty gradient through the burst compared to previous days. Recovered after moving the RF phase shifter. LAS informed.

Achievements/Observations

• Collected calibration and background data for upcoming user experiment.

X-ray delivery
- 7.0 keV, up to 202 pulses at 564 kHz, 1.0 mJ.
- Average pulse energy was about 1.9 mJ on Tuesday and Wednesday. It has to be discussed with BKR tomorrow morning.

Optical laser delivery
- ns laser for jet illumination

Achievements/Observations
- BG measurement with water, buffer low salt
- Lysozyme measurement for geometry file
- Data collection for six different sample concentrations [2 x 15 minutes runs]

Issues
- Pulse energy is very low as compared with Tuesday and Wednesday in this week.
- Damage found on IRU_SLIT4 Top and Bottom blades.
- NKB focus moved by ~20um at around 15:00 (during the handover period). SideMic X moved +20um to compensate it.

X-ray delivery
- 7.0 keV, up to 202 pulses at 564 kHz, 1.0 mJ.
- X-ray beam pointing changed at around 18:12 and it affects nano KB focus (from ~200nm to ~1um).

Optical laser delivery
- ns laser for jet illumination

Achievements/Observations
- Detector moved the most upstream position (~1.5 m sample to detector distance)
- BG measurement with water, buffer low salt
- Silver Behenate measurement for geometry file (mostly for detector distance)
- Data collection for different sample (pure) concentrations

X-ray delivery

• 7.0 keV, up to 202 pulses at 564 kHz, 1.0 mJ.

Optical laser delivery

• ns laser for jet illumination

Achievements/Observations

• Data collection for user sample through column

Issues

• Pressure spike while rotating nozzle tripped AGIPD
• Temperature of ASICs of Q2M1 module too low and not easy to turn it on (issue solved after changing the bath temperature to -27 degreeC)
• Julabo chiller issue again (In the end, set temperature changed to -29.5 degreeC and continued the experiment)
• Another 2 ASICs in Q2M2 and Q2M3 seem unhappy

**X-ray delivery**

• 7.0 keV, up to 202 pulses at 564 kHz, 1.0 mJ.

**Optical laser delivery**

• ns laser for jet illumination

**Achievements/Observations**

• Data collection completed for all the requested samples from user.

**Issues**

• Run repeater behave once abnormally.  Run repeater started with 30 minutes duration, but the first run (run #238) stopped after 40 seconds and next run (run #239) started.

X-ray delivery
- 9.22 and 11.0 keV, 1-352 pulses @ 1.1 MHz, 600-1400 uJ.
- Large intensity gradient with long trains (>70% drop with 352 pulses @ 1.1 MHz).
- Very unstable delivery from 20:30 until 23:00.

Optical laser delivery
- 800 nm, 50 fs, 1-113 pulses @ 564 kHz.
- Stable delivery

Achievements/Observations
- Instrument alignment.
- AGIPD timing scan.
- AGIPD flat field measurement at 1.1 MHz.

Issues
- Twice more time required to collect AGIPD flat fields due to large intensity gradient in the train.
- XTD2 1.2 mm CVD unusable. Initially stuck in the beam, but could be retracted with the help of DOC/PLC OCD.

X-ray delivery

• 11.0 keV, 1-352 pulses @ 1.1 MHz, 600-1100 uJ.
• Even larger intensity gradient with long trains than yesterday.

Optical laser delivery

• 800 nm, 50 fs, 1 pulse.
• Stable delivery.

Achievements/Observations

• Finished AGIPD programme.
• Started JUNGFRAU programme.

Issues

• Poor beam delivery with more than a few bunches per train.

X-ray delivery

• 11.0 keV, 1-351 pulses @ 1.1 MHz, 300-1100 uJ.
• Continuously decaying average intensity through the day.
• Large intensity gradient with long trains.

Optical laser delivery

• 800 nm, 50 fs, 1-113 pulses @ 564 kHz.
• Stable delivery.

Achievements/Observations

• Completed detector programme.

Issues

• Difficulties with AGIPD online calibration. Solved by DOC/CAL.

The SASE1 HIREX interlock is not working as expected.

At the position 'OUT' (step 2 in HIREX scene) and while none of the motors are moving, the interlock SA1_XTD9_HIREX/VDCTRL/HIREX_MOVING is triggered, which prevents the use of more than two pulses.

SA1_XTD9_HIREX/VDCTRL/HIREX_MOVING remains in INTERLOCKED state while moving HIREX in (expected behaviour) and finally goes to ON state when HIREX is inserted, thus releasing the MODES and MODEM interlocks and allowing normal beam operation.

Summary 06.08 - 10.08

X-ray delivery

• 9.3 keV, 1-352 pulses @ 1.13 MHz and 564 kHz, 1.4-1.8 mJ
• 11.56 keV 1-352 pulses @ 1.13 MHz and 564 kHz, 0.7-1.0 mJ.
• Large impact on SASE1 when SASE3 used pulse on demand at the start of the week. Ok since we were setting up, but would be problematic during measurement.
• Overall stable delivery except for the point above.
• Notable downtimes:
  • Thursday afternoon 08.08, beam down during ~1 hour for a ZZ in XTD9 to fix the monochromator motion.
  • Thursday evening 08.08, beam down during the last 45 minutes of the shift following wavelength change request of SASE3.
  • Friday afternoon 09.08, beam down for ~2 hours due to ZZ to fix communication with a device.
  • Saturday morning 10.08, beam down during 45 minutes due to problems with A5.

Optical laser delivery

• 800 nm, 50 fs, 1-202 pulses @ 564 kHz and 141 kHz.
• Laser delivered from Thursday afternoon, as agreed with LAS. One of the issues addressed, but performances still sub-par and more work is required.

Achievements/Observations

• Collected data for all but one PCS proposals. Sample for last PCS is expected to be delivered to EuXFEL on Monday.
• Setup of HIREX for 9.3 and 11.56 keV.
• Completed laser setup for IHR.
• Established laser/X-ray timing.

Issues

• Multiple issues with the online calibration pipeline. It is regrettable that a new version including breaking/major behaviour changes has been deployed after the bring up days, where everything had been succesfuly tested.
  • Constants failing to load after changing detector configuration in the calibration manager. Hotfixed by CAL OCD.
  • AGIPD double pixels mask not correctly applied. Hotfixed by CAL.
  • Changing number of memory cells in the calibration manager, but without loading new constants, changes drastically what is displayed in the AGIPD corrected preview. DOC informed, fix pending.
  • Independent settings for the different pipeline preview data have been implemented, but not communicated. This is very dangerous for the detectors. We have implemented a workaround to restore the previous behaviour.
  • Difficulties in reliably getting a preview of all AGIPD modules even with settings we used with the previous version of the calibration pipeline.
  • HIREX correctino devices had been renamed in the SASE1 topic, but no information was provided to instruments resulting in missing clone devices in instrument topics.
• Offline calibration throws error for most runs because there are sequence files that contain no valid trains produced at the end of the runs. This is not really a problem and would require a less ambiguous statement in myMdC as this makes it difficult to spot when an actual error occurs. DOC/CAL informed.
• DAMNIT could not be started on non-display Maxwell nodes. It turns out an additional argument is required following the OS update during the summer maintenance period, but this is not documented. The solution was provided by DA OCD.
• Ice detector generating many false positive and sending of report not working. To be addressed with DA on Monday.
• Graphical bug in Karabo Image Graph widget when the same data are displayed in two scenes. More detail will be provided to CTRLS.
• XTD9 PBLM at the nominal 'out' position was not fully out and the beam could still be seen on it.
• HIREX interlocks not working as expected and preventing the use of more than two pulses when HIREX is supposedly extracted from the beam path. Mitigated by the PRC.

X-ray delivery

11.56 keV 202 pulses @0.5 MHz, ~1.0 mJ

some downtime due to fire alarm in the tunnel

Optical laser delivery

800 ns laser for jet visualization

PPLaser for time-resolved data collection

Achievements/Observations

• PPLaser timing and alingment done
• Collected several hours of PYP sample with 30ps laser delay

Issues

• DAMNIT issue solved with OCD DA
• some online calibration issues from before persisted

X-ray delivery

12.40 - 12.82 keV, ~1.1 mJ

Optical laser delivery

800 ns laser for jet visualization

Achievements/Observations

• 800 ns laser for jet visualization (aligned but not timed)
• Jungfrau timing done
• IRDa focus done
• IRDa fully aligned
• Sample delivery ready
• Powder data collected

X-ray delivery

12.40 - 12.82 keV, ~1.1 mJ

Optical laser delivery

ns laser for jet visualization
ns laser for pumping ready but not used

Achievements/Observations

• Focus IRD
• ns time and spatial overlap
• Collected lyzo data
• Collected dark rhodopsin data
• New opaque foil installed on cube X-ray exit side

Issues

• Roadrunner motor issues solved after manual intervention and computer restart

X-ray delivery

-12.40 - 12.82 keV, XDT9 XGM ~0.81 mJ@ end of shift

Optical laser delivery

-800 nm laser for jet visualization
-487 nm ns laser for pumping

Achievements/Observations

-Focus IRD
-Collected 10 ns SFX data

Issues

-AGIPD chiller was down

X-ray delivery

-12.40 - 12.82 keV, XDT9 XGM ~0.85 mJ, 3 hours interruption by vacuum issue on XTD9

Optical laser delivery

-800 nm laser for jet visualization
-487 nm ns laser for pumping

Achievements/Observations

-Focus IRD
-Collected SFX data
 

Issues

-AGIPD chiller was down
-Issue with tunnel vacuum valves, at around 7 pm, ended shift early

X-ray delivery

-12.40 - 12.82 keV, ~1.3 mJ

Optical laser delivery

-800 nm laser for jet visualization
-525 nm ns laser for pumping

Achievements/Observations

-Focus IRD
-Collected SFX data

Issues

-SPB_EHC_VAC/DCTRL/GAUGE_FR_1_Value triggered interlock, we could not open gate valve : SPB_IRU_VAC/VALVE/VALVE_INLINE_3

X-ray delivery

• 12.78 keV, ~1.3 mJ

Optical laser delivery

• 800 nm laser for jet visualization

Achievements/Observations

• Collected SFX data
• Calibration date for HIREX measured (at different X-ray energy)

X-ray delivery

12.8 keV, ~0.8 mJ

Achievements/Observations

- Data collection with fixed target

Issues

- M1 and M2 position on SPB/SFX Setpoint J was far from optimal
- Beam position in X was drifting to minus direction all time