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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 10 of 24  Not logged in ELOG logo
Entry   Shift summary, posted by Romain Letrun on 03 Jun 2023, 23:40 
X-ray delivery


10.65 keV, up to 339 pulses at 1.13 MHz, 1.6-1.8 mJ.
12.4 keV, up to 30 pulses at 1.13 MHz, 1.0-1.2 mJ.
Beam not
aligned to the crosshair at 12.4 keV, but we could work with it as it is to avoid further tuning.
Overall stable delivery.


Optical
Entry   Shift summary, posted by Konopkova Zuzana on 04 Jun 2023, 14:53 
beam parameters: 20 keV, 300 uJ, 352 pulses


continuation of user programe.
Machine performance very good for trying the 20 keV the first time. Experiment also going well.
Entry   Shift summary, posted by Romain Letrun on 04 Jun 2023, 21:17 
X-ray delivery


12.2-12.45 keV, up to 339 pulses at 1.13 MHz, 0.8-1.2 mJ.
Couple of minutes beam interruption.


Optical
laser delivery
Entry   Shift summary, posted by Ulrike Boesenberg on 09 Jun 2023, 02:22 
*Vacuum issues: There seems to be a leak in the arm nr. 6 (2.4mm CVD Diamond). This has escalated to trip several times the vacuum sector interlock.
VAC will do an intervention to XTD1 with broken interlock tomorrow morning starting 9am to remove arm 6 permanently and putting a blind flange instead. 
*We can measure for today with the 2.4mm CVD Diamond inserted into the beam.
Entry   Shift summary, posted by Adam Round on 09 Jun 2023, 07:05 
Staff: DZ, AR, MK

X-ray delivery


12.42 keV 169 pulses for alignment 16 pulses for data collection. stable delivery excluding the extended interuption


Optical
Entry   Shift summary, posted by Ulrike Boesenberg on 10 Jun 2023, 00:39 
* Data collection of vycor and glass samples in SAXS geometry until 9am

* Successful intervention on SA2_XTD1_ATT arm 6 by the vacuum group, see elog entry 237 by Raoul and Bianca . Thanks!

* Simultaneous CoC in the MID hutch to WAXS geometry.
Entry   Shift summary, posted by Chan Kim on 10 Jun 2023, 06:55 
X-ray delivery


12.42 keV, 0.8 mJ/pulse, stable delivery


Optical laser delivery


none


Achievements/Observations
Entry   Shift summary, posted by Ulrike Boesenberg on 11 Jun 2023, 02:08 
* First half of the day was used to optimize seeding performance
* Cryo issues started at 6 pm; were resolved by 9:30pm
* After some tuning, we observed very nice seeding performance around midnight (ratio better than 1:1)
Entry   Shift summary, posted by Chan Kim on 11 Jun 2023, 07:28 
X-ray delivery


12.42 keV, 0.65 mJ/pulse, low pulse energy but mostly stable delivery


Optical laser delivery


none


Achievements/Observations
Entry   Shift summary, posted by Ulrike Boesenberg on 12 Jun 2023, 02:01 


*Some more tuning of HXRSS and focus optimization in the morning.

*XPCS data taken in WAXS geometry on different glass samples.
Entry   Shift summary, posted by Chan Kim on 12 Jun 2023, 07:16 
X-ray delivery


12.42 keV, stable delivery with slightly less than 1.0 mJ/pulse (~0.95 mJ/pulse)


Optical laser delivery


none


Achievements/Observations
Entry   Shift summary, posted by Konopkova Zuzana on 13 Jun 2023, 23:08 
beam: 18 keV, 352 pulses, ~200 uJ per pulse

achievements:


AGIPD timing scans, AGIPD darks.
beam alignment, CRL3 focusing, prep for the user beamtime


beam conditions:
Entry   Shift summary, posted by Konopkova Zuzana on 15 Jun 2023, 06:41 
18 keV, 150 uJ per pulse, 2.2 MHz


continuing user program proposal 3285
X-ray heating and laser heating samples in DACs
using only the first 200
pulses of the train as the intensity after decreases fast, conversion of the samples is difficult due to low pulse energies
Entry   Shift summary, posted by Johan Bielecki on 15 Jun 2023, 23:08 
X-ray delivery


12.42 keV, stable delivery in single pulse mode with 1.9 mJ/pulse


Optical laser delivery


532 nm ns-laser for sample pumping


Achievements/Observations
Entry   Shift summary, posted by Konopkova Zuzana on 17 Jun 2023, 07:27 
Beam 18 keV, 0.5 MHz, long trains up to ~280 pulses


change setup to dynamic DAC
prep for user beamtime: alignment of X-rays, focusing (~40 um), train-on-demand for long trains,
transmission runs
darks, XRD calibrations for AGIPD


Issues:
Entry   Shift summary, posted by Konopkova Zuzana on 19 Jun 2023, 05:34 

concluded user experiment on dynamically compressed water
long train operation worked relatively stable with no major interuptions
in beam delivery
Entry   Shift summary, posted by Ulrike Boesenberg on 30 Jul 2023, 02:02 
9.3 keV, 1-35pulses, stable delivery ~600uJ
*General alignment of MID branch to the DES
*Commissioning of CRL2 (MID_XTD6_CRL) together with EEE after change to close loop in the maintenance period and alignment of lenses, characterization
Entry   Shift summary, posted by Ulrike Boesenberg on 30 Jul 2023, 23:06 
9 and 10keV beam, up to 30 bunches, significant drop in intensity in the morning and in the evening.

Activities:

Commissioning of EH MIRR device
Entry   Shift summary, posted by Romain Letrun on 05 Aug 2023, 08:20 
X-ray delivery


9.3 keV, 1-202 pulses at 1.13 MHz, 1.9-2.1 mJ.
Overall stable delivery.
L-IBFB could not be activated due to missing
missing transfer matrix elements. Missing parameters entered by the expert who happened to be on shift this morning.


Optical
Entry   Shift summary, posted by Ben, Justine on 05 Aug 2023, 15:33 
Achievements


Measured XAS and RIXS from NdNiO3 test sample at 230 K


Plan for next shift


Measure test sample at 20K
Find timing between X-ray and laser and look for transient signal
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