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Experiment data
OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn
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Message ID:
255
Entry time:
15 Jun 2023, 23:08
Author:
Johan Bielecki
Group:
SPB
Subject:
Shift summary
X-ray delivery
12.42 keV, stable delivery in single pulse mode with 1.9 mJ/pulse
Optical laser delivery
532 nm ns-laser for sample pumping
Achievements/Observations
Collected protein crystal diffraction for three different samples with varying laser delay and fluence. LCP viscous jet sample delivery.
Stable CRL focus using tunnel collimation with 3 XTD2 lenses followed by 17 focusing lenses in SPB hutch. 2 um FWHM focus with <1um standard deviation in 'X' position.
3 XTD2 lenses gives a round X-ray beam approx 1 mm in size, such that we are almost overfilling the CRL apertues in SPB.
Issues
Some initial jetting issues, which have now been solved.
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