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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 19 of 24  Not logged in ELOG logo
ID Date Author Groupdown Subject
  281   30 Jul 2023, 02:02 Ulrike BoesenbergMIDShift summary

9.3 keV, 1-35pulses, stable delivery ~600uJ
*General alignment of MID branch to the DES
*Commissioning of CRL2 (MID_XTD6_CRL) together with EEE after change to close loop in the maintenance period and alignment of lenses, characterization of beamsize using the X-ray eye at the sample position.
*Alignment of spectrometer in DES

  283   30 Jul 2023, 23:06 Ulrike BoesenbergMIDShift summary

9 and 10keV beam, up to 30 bunches, significant drop in intensity in the morning and in the evening.

Activities:

Commissioning of EH MIRR device

Preparation of user experiment at 10keV with lenses and monochromator

  294   09 Aug 2023, 01:42 Jörg HallmannMIDShift summary
  • after alignment of the beam, the main topic of the day were flatfields for the AGIPD with various settings
  • corresponding darks have been taken in addition
  •  
  • it was challenging to generate proper flatfield intensities on the detector (1photon peak equally high as the 0photon peak) due to the low intensity (750uJ)
  • shift crew received a warning of the machine that using the required 352 pulses for longer time could lead to an overheating of components in the machine -> flatfields were generated by using 172 pulses and sticking them together by shifting the delay
  295   10 Aug 2023, 01:31 Jörg HallmannMIDShift summary

- finalized the flatfields of the AGIPD at 0.5 MHz
- optimized the performance of the beam (now 850 - 950 uJ)
- measured flatfield and darks for the Jungfrau detector
- optimized the instrument alignment of FEL beam and ALAS to the center of rotation
 

  298   11 Aug 2023, 01:44 Jörg HallmannMIDShift summary

alignment checks of the CRL2 device as well as the Mono - continuation of both devices together planned for tomorrow
flatfelds for EPIX & AGIPD (needed to be redone because of too low intensity during the previous measurements)
installation of the levitation device and first test measurements

 

  300   12 Aug 2023, 01:32 Jörg HallmannMIDShift summary

measured various sample using the levitation device

issues:
during the change of the sample detector distance, the AGIPD chiller "Julabo" switch itself off and went into error - on & off procedure solved the problem and need further investigation

  321   25 Aug 2023, 06:20 Johannes MoellerMIDShift summary

Shift summary the 24th of Aug

  • MID takes the seeded beam about 200 uJ including SASE background.
  • Monochrometer is aligned.
  • Mono + CRL2 was tested.
  • Found rough timing with a fast diode at the sample position
  • Finding the temporal overlap with Forsted YAG hasn't been done yet. The motor (PPODL) doesn't change the laser delay, but LA2_LAS_PPL/CTRL/TRGDLY does. The values is not able to implemented into the Scantool since it doesn't have target position.
  • Photon energy spectrum was measured w and w/o mono with Gotthard at DES.
  • Nano focusing lens is aligned. The beam size is about 20 um X 20 um. Very stable pointing at the sample position.
  324   26 Aug 2023, 02:07 Felix BrausseMIDShift summary

Shift summary the 25th of Aug

  • Found laser and X-ray spatiotemporal overlap with Bi diffraction peak
  • Found a diffraction peak from STO nano particles
  • X-ray dose test is ongoing

  • EXP_UPP_T10 was stuck at the hardware limit but the encoder value shows different values.

  • Cryo Failure at 1:30 am; BKR called and predicted ~20 hrs of downtime

  328   28 Aug 2023, 02:14 Wonhyuk JoMIDShift summary

Shift summary for 28th of Aug.
- Realigned the center of rotation. 
- MID took the seeded beam at about 120 uJ around 4 p.m. after the long intervention.
- Cross-checked the time zero with Bi 222 diffraction peak.
- Searching and collecting diffraction patterns from a single nanocrystal. 
The user will continue to find the optimized condition for the flux of X-ray and Laser. 

 

  330   29 Aug 2023, 03:14 Wonhyuk JoMIDShift summary

Shift summary for 29th of Aug.

- Conducted Time-resolved Bragg CDI experiment using 3rd harmonic pump laser. 
- Collected coherent diffraction patterns from Perovskite-oxide nanocrystals for various time delay and laser fluence. 
- Checked the correlations between the XGM, diamond detector in SDL, and two Jungfrau detectors running on interleave mode. 

  372   29 Sep 2023, 00:35 Johannes MoellerMIDShift summary

1, 60 and 350 pulses at 8.7keV, HXRSS

*focus characterization CRL2 lens 3,5,6
*Si 20nm XPCS with 20 and 50 pulses to evaluate the contrast
*damage and dynamic studies on HGW with 1 and 350pulses and different attenuation and different temperatures

HXRSS tuning is ongoing during the night, we leave the beam on the MID spectrometer and the zoom session open for tuning.
 

  378   01 Oct 2023, 02:00 Johannes MoellerMIDShift summary

HXRSS at 8.8 keV, 1, 60 or 350 pulses. Quite stable seeding performance

  • loaded new sample (HGW) in the morning
  • measured full temperature series on HGW during the day
  • problem with vacuum in the cryostat-chamber, which triggered the interlocked during the data taking and blocked AGIPD for some temperatures
  • focussing optimized in the evening and relaxing the bender, with 2-3 times better contrast determined. Please don’t touch CRL2 from now.
  • loaded new sample in the evening, but insufficient vacuum in the user chamber prevents opening the valve to the AGIPD first
  393   18 Oct 2023, 02:09 Alexey ZozulyaMIDShift summary

Shift summary (p4239)
Achievements:
- HXSS beam at 10.5 keV at 400 uJ pulse energy
- MID beam alignment to DES
- aligned DES spectrometer for C220 reflection on Gotthard and flight path;
Issues:
-    Seeding crystal was stuck in parked position and could not be inserted back (late evening); to be investigated via ZZ access tomorrow

  405   23 Oct 2023, 01:10 Alexey ZozulyaMIDShift summary

Milestones:
*Finish measurement program on the STO sample at room temperature
*Check mono fpitch and energy rocking curve
*Darks for AGIPD and JF
*take out mono, CRLs etc from the tunnel

Beam delivery:

*Beam was not available from 11:30 to 19:30. Returned to good conditions back at  ~2mJ, 10.5keV, 15bunches

 

  428   01 Nov 2023, 02:22 Johannes MoellerMIDShift summary
  • stable delivery of 1mJ at 18keV SASE
  • succesful beamline alignment for MID (CRLs + M1 and M2) with mono.
  • alignment of NAFO stack to DES and zyla camera with SASE and monochromatic beam
  • setup of DES spectrometer for 18keV on 440 reflection with SASE
  • timing of PP laser with perpendicular excitation condition with diode and YAG

Problems:
Mirror M2 needs 30min to move from SASE to Mono position

  430   02 Nov 2023, 02:28 Johannes MoellerMIDShift summary
  • stable delivery of 1mJ SASE at 18keV
  • NAFO lens characterization with caustic scan
  • successful detector calibration of AGIPD with LaB6 and alignment of Jungfrau to diffraction signal with LaB6
  • test of ptychography with 18keV (not successful)
  • successful setup of online holography analysis with test measurements
  434   04 Nov 2023, 02:29 Johannes MoellerMIDShift summary
  • Stable delivery of SASE at 18 keV. The intensity dropped slightly from 1mJ to 0.88mJ during the evening, but everything good.
  • fixed the laser pulse-on-demand + FSSS scanning macro
  • We take some images series of the laser drilling process for different laser fluences
  • We started to take first time resolved data
  437   05 Nov 2023, 04:08 Angel Rodriguez FernandezMIDShift summary
  • stable SASE beam delivery with 1mJ pulse energy
  • we took data for different optical laser excitation fluences and delays
  • we changed from the optical lock to the electronic lock to measure also longer delays.
  453   22 Nov 2023, 10:19 Johannes MoellerMIDIssue

The Si 0.5mm absorber of XTD1 attenuator seems to be damaged. First screenshot is with that one inserted. In the second screenshot, it is replaced with a Si 0.5mm from MID_XTD6_ATT.

 

Attachment 1: Screenshot_from_2023-11-22_10-15-34.png
Screenshot_from_2023-11-22_10-15-34.png
Attachment 2: Screenshot_from_2023-11-22_10-14-47.png
Screenshot_from_2023-11-22_10-14-47.png
  454   22 Nov 2023, 22:48 Johannes MoellerMIDShift summary

*Tests for online XPCS pipeline ongoing
*beam optimization with power slits, current beam size 8x13um (v x h), we assign the larger value in the horizontal direction to jitter
*Movement of the AGIPD quadrants to increase q range to lower values
*analysis and update of Sample to detector distance and geometry
*ScannerX of the FSSS is crashing very! frequently.

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