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  OPERATION-2023 logbook, Contact: F.Wolff-Fabris, A.Galler, L.Samoylova, H.Sinn, Page 18 of 24  Not logged in ELOG logo
Entry   Issue, posted by Yifeng Jiang on 07 Apr 2023, 23:57 2023-04-07-235513_774809068_exflqr51474.png
After receiving beam from SPB, we noticed that there is a werid shape of beam in the FEL imager which was not observed yesterday.

Maybe someone left X-ray component in the beam.
Entry   Shift summary, posted by Johan Bielecki on 07 Apr 2023, 23:03 
Beam delivery for proposal 3378

Achievements/Observations


Collected data on liquid H20 and D20
Found conditions where only ice were seen. approx. 4h of ice data taken. Starting to
Entry   HED Shift Summary 07.04., posted by Alejandro Laso Garcia on 07 Apr 2023, 23:00 
Morning - Users from proposal 3455 continued with their measurement program. Beam stable during the measurements.

Afternoon - Changed the setup from 3455 to 3326.

Evening - Beginning of the alignment for users. Beam stable.
Entry   XTD2 Si500 attenuator broken, posted by Johan Bielecki on 04 Apr 2023, 11:18 Screenshot_from_2023-04-04_11-17-46.pngScreenshot_from_2023-04-04_11-18-04.png
Attachment 1: Beam in SPB hutch with Si500

Attachment 2: Beam without Si500
Entry   Issue, posted by Frederik Wolff-Fabris on 04 Apr 2023, 08:37 
TUE 08:30AM:

The SA3 Cell 17 & 18 Phase shifters do not move and encoders are damaged. A ZZ is needed to exchange the encoders. Instruments are informed
and access will take place Tuesday morning. Machine has separated the north branch.
Entry   Summary day shift 2023-04-04, posted by Lisa Randolph, Carsten Baehtz, Alexander Pelka on 04 Apr 2023, 07:11 FEL_imager_2023-04-04_08-09-58.png
04 Apr 2023, 07:44 we realize that the SetpointsHED Macro lost all values, probably during the Karabo Crash. Since it is a macro, the values arent stored
anywhere. DOC tries to recover. Meanwhile, we found the values for 3mrad, 2.5mrad and 2mrad in old screenshots and update the macro values from that. Saving
those now locally in nextcloud/user/Alex.
Entry   Night shift summary 02.04.2023, posted by Loic, Yi-Ping on 03 Apr 2023, 06:38 
Achievements:

Collected more scans on cyanocobalamin, both delays scans and dynamic XAS

Issues with bad signal in beginning but good signal in the last hours
Entry   Late Shift Summary, posted by Benjamin van Kuiken on 02 Apr 2023, 04:46 
Achievement


Measured tXAS at the Fe L-edge of Fe(bpy)3 using both delay and energy scans. 


Issues


The cold traps ran empty on the chamber resulting in a pressure spike that interlocked the DSSC
The rough vacuum of the chem
Entry   Shift summary, posted by Tokushi Sato on 01 Apr 2023, 06:51 
X-ray delivery


1-202 pulses, 564 kHz, stable delivery
Beam was down from 06:08


Optical laser delivery


800nm, 50 fs, 282 kHz, stable delivery 


Achievements/Observations
Entry   Shift summary, posted by Tokushi Sato on 31 Mar 2023, 06:59 
X-ray delivery


1-202 pulses, 564, 282, 141 , 70.5 kHz, stable delivery


Optical laser delivery


800nm, 50 fs, 282 kHz, stable delivery 


Achievements/Observations
Entry   Late Shift Summary, posted by Benjamin, Yi-Ping, Ru-Pan, Andreas on 31 Mar 2023, 05:10 
Achievements


Optimized BOZ for Co and Fe
Estabilished Stable liquid jet flow with 30 mM Fe(bpy)3


Problems


Jet froze several times
Chamber warmed up earlier in the day. This led to a "dusting" of CNCbl on many surfaces
Entry   shift summary March 30th, posted by Jörg Hallmann on 31 Mar 2023, 01:51 
- seeding at ~800 uJ

- repaired the laser interlock of A.08

- EPIX back in operation
Entry   Shift summary, posted by Tokushi Sato on 30 Mar 2023, 06:53 
X-ray delivery


1-202 pulses, 564, 282, 141 kHz, stable delivery


Optical laser delivery


800nm, 50 fs, 282 kHz, stable delivery


Achievements/Observations
Entry   Shift Summary, posted by Benjamin, Robert, Yi-Ping, Ru-Pan on 30 Mar 2023, 04:16 
Achievements


Found coarse timing between XFEL and optical laser


Problems


Did not see a observe fine timing signal from silicon nitride measurement


Plan for night shift
Entry   shift summary March 29th, posted by Jörg Hallmann on 30 Mar 2023, 02:37 
achievments: alignment of the SDL (both branches)

measuring of samples & calibrants

 
Entry   Shift summary March 28th, posted by Jörg Hallmann on 29 Mar 2023, 01:31 
Seeding at 9 keV with 800 - 1000uJ intensity

1. alignment of the lower branch of the SDL

2. focussing with CRL2 and check of the beam size using wire scans (slightly more than 10 um)
Entry   Issue, posted by Angel Rodriguez Fernandez on 28 Mar 2023, 15:26 IMG_8399.JPG
The door from MID side entrance was smashed and we lost the radiation permit.

The acciedent happened between 11 (when the door was lest use by MID members) and 14:19 (when the picture was taken).

It is possible that we will have the permit in the next hours to countinue.
Entry   Shift end, posted by Jayanath Koliyadu on 26 Mar 2023, 23:27 
X-ray delivery


1-165 pulses, 1.1 MHz - 56.4 kHz, upto 350  uJ @ 50 pC


Optical laser delivery


ns laser for imaging


Achievements/Observations
Entry   Status, posted by Naresh Kujala on 26 Mar 2023, 13:26 
Machine RC Raimond informed PRC that there is an issue with the A4 module that needs to fix to have a continuous operation. To fix this they need
20 min.

Agreed with all instruments (SPB, SQS, and HED) that at 13:30hr machine will take over the beam for 20 min.
Entry   Shift end, posted by Jayanath Koliyadu on 25 Mar 2023, 23:18 
X-ray delivery


1-165 pulses, 1.1 MHz - 56.4 kHz, upto 350  uJ @ 50 pC


Optical laser delivery


ns laser for imaging


Achievements/Observations
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